Towards eco‐friendly secondary plant metabolite quantitation: Ultra high performance supercritical fluid chromatography applied to common vervain ( Verbena officinalis L.)

Two new iridoids from Verbena officinalis L.

Two new iridoids, 3-(5-(methoxycarbonyl)-2-oxo-2H-pyran-3-yl)butanoic acid, named verbeofflin I (1), and 7-hydroxydehydrohastatoside (2), were isolated from the aerial part of Verbena officinalis L, along with three known iridoids, verbenalin (3), 3,4-dihydroverbenalin (4), hastatoside (5) by means of various column chromatography steps. The structures of these compounds were elucidated through...

Ultra‐high performance supercritical fluid chromatography of lignin‐derived phenols from alkaline cupric oxide oxidation

Traditional chromatographic methods for the analysis of lignin-derived phenolic compounds in environmental samples are generally time consuming. In this work, an ultra-high performance supercritical fluid chromatography method with a diode array detector for the analysis of major lignin-derived phenolic compounds produced by alkaline cupric oxide oxidation was developed. In an analysis of a col...

High Performance Carbon Dioxide Recycling for Supercritical Fluid Chromatography

Supercritical Fluid Extraction+supercritical Fluid Chromatography

high pressures also requires special equipment. In summary, both RESS crystallization and SAS crystallization appear to be promising methods for generating supersaturation and therefore represent alternatives to conventional crystallization. Such alternatives may prove attractive in applications such as polymer and pharmaceutical processing, or in particle design for drug delivery. It is possib...

Volatile Constituents from the Aerial Part of Verbena Officinalis L. (Vervain)

The volatile constituents of the aerial parts of vervain (Verbena officinalis L.) cultivated locally were investigated. Analysis of the volatile fraction by GC and GC-MS is described. Compounds were identified by various methods, the major compounds being 3-hexen-1-ol (7.28%), 1-octen-3-ol (32.76%), linalool (4.66%), verbenone (20.49%) and geranial (7.22%).